六氟化硫气体质量现场一体化检测技术及装置研发

张晓琴; 杜子韦华; 朱洪斌; 余翔; 孙磊

doi:10.13296/j.1001-1609.hva.2026.08.026

您当前的位置：

首页 >

文章列表页 >

六氟化硫气体质量现场一体化检测技术及装置研发

技术讨论 | 更新时间：2026-08-12

- 六氟化硫气体质量现场一体化检测技术及装置研发
- Research and Development of On-site Integrated Detection Technology and Device for Sulfur Hexafluoride Gas Quality
- 高压电器 2026年62卷第8期页码：222-229
- 作者机构：
  
  国网江苏省电力有限公司电力科学研究院，南京 211103
- 作者简介：
  
  张晓琴（1989—），女，硕士研究生，从事电力绝缘介质智能化分析方法研究（通信作者）（E-mail：15850736276@126. com）。
- 基金信息：
  
  国网江苏省电力有限公司科技项目Science and Technology Project of State Grid Jiangsu Electric Power Co., Ltd.(J2024104)
- DOI：10.13296/j.1001-1609.hva.2026.08.026
  中图分类号：
- 收稿：2025-01-09，
  
  修回：2025-09-22，
  
  纸质出版：2026-08-16
- 稿件说明：
移动端阅览
张晓琴, 杜子韦华, 朱洪斌, 等. 六氟化硫气体质量现场一体化检测技术及装置研发[J]. 高压电器, 2026,62(8):222-229.

ZHANG Xiaoqin, DU Ziweihua, ZHU Hongbin, et al. Research and Development of On-site Integrated Detection Technology and Device for Sulfur Hexafluoride Gas Quality[J]. High Voltage Apparatus, 2026, 62(8): 222-229.
张晓琴, 杜子韦华, 朱洪斌, 等. 六氟化硫气体质量现场一体化检测技术及装置研发[J]. 高压电器, 2026,62(8):222-229. DOI： 10.13296/j.1001-1609.hva.2026.08.026.

ZHANG Xiaoqin, DU Ziweihua, ZHU Hongbin, et al. Research and Development of On-site Integrated Detection Technology and Device for Sulfur Hexafluoride Gas Quality[J]. High Voltage Apparatus, 2026, 62(8): 222-229. DOI： 10.13296/j.1001-1609.hva.2026.08.026.

摘要

气体具有优异的绝缘、灭弧性能，广泛应用于超、特高压气体绝缘开关、封闭式组合电器等设备中。文中针对SF

气体全分析耗时长、步骤繁琐、无法在变电站现场开展等难题，首创了SF

气体酸度、可水解氟化物、矿物油含量仪器化检测方法，创新了纯度、水分、毒性物质小型化稳流分析方法，发明了6项质量指标并行全自动检测方法及装置，实现了SF

气体质量的现场精确快速检测。采用文中研发的方法及装置，单个SF

气体样品检测时间由18 h缩短至40 min，检测用气量由100 L减少至20 L，且避免了SF

高压钢瓶在现场与实验室之间来回运输，对保证重大工程建设周期、保障充气设备可靠运行具有重要意义。

Abstract

gas is widely used in such equipment as extra and ultra-high-voltage gas insulated switchgear and gas insulated metal enclosed switchgear due to its excellent insulation and arc interruption performance. To address the challenges of time-consuming procedures

cumbersome steps and the infeasibility of on-site analysis at substation for comprehensive SF

gas analysis

in this paper the instrumental detection methods for SF

gas acidity

hydrolyzable fluorides

and mineral oil content are poineered. The miniaturized steady-flow analysis methods for purity

moisture

toxic substances are innovated

the parallel fully automated detection method and device for six quality indicators are invented and the accurate and rapid on-site detection of SF

quality is achieved.With the use of method and device developed in this paper

the detection time of single SF

gas sample is reduced from 18 h to 40 min

the detection gas consumption is reduced from 100 L to 20 L

and the bck-and forth transportation of high pressure SF

cylinders between the site and the laboratory is eliminated. This is of great significance for ensuring the construction schedule of major projects and guaranteeing the reliable operation of gas-filled equipment.

关键词

Keywords

references

曾福平,朱可馨,冯孝轩,等. SF 6 故障分解及特征组分检测研究进展[J ] .高电压技术,2023,49(8):3240-3257.

Zeng Fuping, Zhu Kexin, Feng Xiaoxuan, et al.Progress in SF 6 decomposition and detection of its characteristic decomposition components[J ] . High Voltage Engineering,2023,49(8):3240-3257.

尹凯强,陈功,安韵竹,等.气压和温度对SF 6 气体绝缘性能的影响[J ] .电瓷避雷器,2023,23(2):71-77.

Yin Kaiqiang, Chen Gong, An Yunzhu, et al.Influence of pressure and temperature on SF 6 insulation performance[J ] . Insulatators and Surge Arresters,2023,23(2):71-77.

王秀君,罗林,于淼,等.基于马尔可夫转移场的SF 6 分解气体紫外吸收光谱检测[J ] .浙江电力,2025,44(3):116-124.

Wang Xiujun, Luo Lin, Yu Miao, et al.Detection of SF 6 decomposition gases using ultraviolet absorption spectroscopy based on Markov transition fields[J ] . Zhejiang Electric Power,2025,44(3):116-124.

陆淼,吴欣烨,胡海敏,等.SF 6 变压器气体冷却循环风机智能监测系统[J ] .变压器,2024,61(12):61-67.

Lu Miao, Wu Xinye, Hu Haimin, et al.SF 6 transformer gas cooling circulating fan intelligent monitoring system[J ] . Transformer,2024, 61(12):61-67.

李昊天,曾福平,颜伊鸣,等.Ag表面对SF 6 初级分解产物氧化反应的影响作用研究[J ] .电工技术学报,2024,39(9):2841-2850.

Li Haotian, Zeng Fuping, Yan Yiming, et al.Study on the effect of Ag surface on Oxidation of SF 6 primary decomposition products[J ] . Transactions of China Electrotechnical Society,2024,39(9):2841-2850.

唐炬,杨东,曾福平,等.基于分解组分分析的SF 6 设备绝缘故障诊断方法与技术的研究现状[J ] . 电工技术学报,2016,31 (20):41-54.

Tang Ju, Yang Dong, Zeng Fuping, et al. Research status of SF 6 insulation equipment fault diagnosis method and technology based on decomposed components analysis[J ] . Transactions of China Electrotechnical Society,2016,31(20):41-54.

马径坦,张乔根,游浩洋,等. SF 6 电气设备中微水对固体绝缘材料闪络电压的影响[J ] . 高电压技术,2018,44(6):1822-1827.

Ma Jingtan, Zhang Qiaogen, You Haoyang, et al. Influence of moisture on flashover voltage of solid insulating materials in SF 6 electrical equipment[J ] . High Voltage Engineering,2018,44(6):1822-1827.

马凤翔,赵跃,赵新瑜,等.基于紫外光声光谱的SF 6 特征分解组分SO 2 的高灵敏度检测技术[J ] . 光子学报,2023,52(3):198-206.

Ma Fengxiang, Zhao Yue, Zhao Xinyu, et al. High sensitivity detection technology of SF 6 characteristic decomposition component SO 2 based on UV photoacoustic spectroscopy[J ] . Acta Photonica Sinica,2023,52(3):198-206.

Okubo H, Beroual A. Recent trend and further perspectives in electrical insulation techniques in relation to SF 6 substitutes for high voltage electric power equipment[J ] . IEEE Electrical Insulation Magazine,2011,27(2):34-42.

徐长福,赵新冬,梁伟,等.基于数字孪生技术的GIL综合管廊气体泄漏与排除全过程风险性评估[J].电力系统保护与控制, 2025,53(3):160-171.

Xu Changfu, Zhao Xindong, Liang Wei, et al.Risk assessment of gas leakage and elimination in GIL utility tunnels based on digital twin technology[J]. Power System Protection and Control,2025,53 (3):160-171.

张博雅,唐念,孙东伟,等.新型SF 6 替代气体全氟甲基乙烯基醚的绝缘性能研究[J ] .高压电器,2025,61(2):165-170.

Zhang Boya, Tang Nian, Sun Dongwei, et al.Research on insulation performance of a newCF 3 OCF=CF 2 alternative gas to SF 6 [J ] . High Voltage Apparatus,2025,61(2):165-170.

谢声益,吴芳芳,朱珉,等.三相共箱气体绝缘输电线路多物理场数值仿真分析[J].浙江电力,2025,44(8):111-118.

Xie Shengyi, Wu Fangfang, Zhu Min, et al.Numerical simulation and analysis of multi-physics fields in three-phase enclosed GIL[J]. Zhejiang Electric Power,2025,44(8):111-118.

王昊,张长虹,杨旭,等. 420 kV及以上高压断路器电寿命试验中SF 6 气体分解产物及其影响研究[J ] . 高压电器,2023,59 (10):88-95.

Wang Hao, Zhang Changhong, Yang Xu, et al. Study on the effect of SF 6 gas decomposition products in electrical endurance test of 420 kV and abov e circuit breaker[J ] . High Voltage Apparatus, 2023,59(10):88-95.

杨韧,张晓,彭雅楠,等. SF 6 断路器开断过程中固体分解产物研究[J ] .高压电器,2022,58(12):21-27.

Yang Ren, Zhang Xiao, Peng Yanan, et al. Study on solid decomposition products during interruption period of SF 6 circuit breaker[J ] . High Voltage Apparatus,58(12):21-27.

GB/T 12022—2025 工业六氟化硫[S].

GB/T 12022—2025 Industrial sulfur hexafluoride[S].

GB/T 8905—2012 六氟化硫电气设备中气体管理和检测导则[S].

GB/T 8905—2012 The guide for management and measuring SF 6 gas in electrical equipment[S ] .

张国治,胡栩焜,邓广宇,等. SF 6 及SF 6 故障分解气体与局部放电柔性特高频天线传感器基底相容性实验研究[J ] . 电工技术学报,2023,38(15):4050-4062.

Zhang Guozhi, Hu Xukun, Deng Guangyu, et al. Experimental study on substrate compatibility of SF 6 and SF 6 fault-decomposing gases with partial discharge flexible UHF antenna sensors[J ] . Transactions of China Electrotechnical Society,2023,38(15):4050-4062.

张利燕,杜黎明,张若飞,等.六氟化硫气体酸度测定干扰因素分析[J]. 河北电力技术,2012,31(3):30-32.

Zhang Liyan, Du Liming, Zhang Ruofei, et al. Influencing factors analysis on sulfur hexafluoride acidity determination[J]. Hebei Electric Power,2012,31(3):30-32.

梁真镇,付梦月,高英武,等.六氟化硫中可水解氟化物的吸附试验及分析[J]. 化学推进剂与高分子材料,2011,9(4):89-90.

Liang Zhenzhen, Fu Mengyue, Gao Yingwu, et al. Adsorption test and analysis of hydrolysable fluorides in sulfur hexafluoride[J]. Chemical Propellants & Polymeric Materials,2011,9(4):89-90.

Van Heyst A, Vanlancker M, Vercammen J, et al. Analysis of mineral oil in food: results of a belgian market survey[J]. Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure&Risk Assessment,2018,35(10):2062-2075.

唐亮.六氟化硫电气设备特征气体气相色谱分析方法的研究[J]. 分析仪器,2016(3):57-60.

Tang Liang. Study on method for determination of characteristic gas in sulfur hexafluoride SF 6 electrical equipment by gas chromatography[J ] . Analytical Instrumentation,2016(3):57-60.

顾琦,仲林林.基于一维电弧模型的SF 6 混合气体灭弧性能评价[J ] . 电力工程技术,2022,41(6):140-146.

Gu Qi, Zhong Linlin. Evaluation of the interruption capability of SF 6 gas mixtures based on one-dimensional arc model[J ] . Electric Power Engineering Technology,2022,41(6):140-146.

陶风波,王帅,贾勇勇,等.特高压气体绝缘金属封闭式组合电器的现场冲击耐压试验方法[J]. 高电压技术,2018,44(12):3936-3943.

Tao Fengbo, Wang Shuai, Jia Yongyong, et al. Method of on-site tests for the withstand voltage of ultra-high-voltage GIS lightning impulse[J]. High Voltage Engineering,2018,44(12):3936-3943.

赵科,王静君,刘通,等.直流GIL绝缘设计及局部放电检测研究进展[J]. 电力工程技术,2017,36(5):98-102.

Zhao Ke, Wang Jingjun, Liu Tong, et al. A review of insulation design and partial discharge detection of DC gas insulated line[J]. Jiangsu Electrical Engineering,2017,36(5):98-102,108.

薛光辉,王一凡,于浩,等.基于恒定应力加速寿命试验的SF 6 气体密度表可靠性研究[J ] . 电测与仪表,2024,61(6):194-202.

Xue Guanghui, Wang Yifan, Yu Hao, et al. Reliability study of SF 6 gas density meter based on constant stress acceleratedlife test[J ] . Electrical Measurement & Instrumentation,2024,61(6):194-202.

赵丽娜,赵丽娟,宁子达,等.一种SF 6 压力指针式仪表的定位识别方法[J ] . 电测与仪表,2025,62(2):210-216.

Zhao Lina, Zhao Lijuan, Ning Zida, et al. A positioning recognition method for SF 6 pressure pointer meter[J ] . Electrical Measurement & Instrumentation,2025,62(2):210-216.

范建斌,李鹏,李金忠,等. ±800 kV特高压直流GIL关键技术研究[J]. 中国电机工程学报,2008,28(13):1-7.

FAN Jianbin, LI Peng, LI Jinzhong, et al. Study on key technology of ±800 kV UHVDC GIL[J]. Proceedings of the CSEE,2008,28 (13):1-7.

齐波,张贵新,李成榕,等.气体绝缘金属封闭输电线路的研究现状及应用前景[J]. 高电压技术,2015,41(5):1466-1473.

Qi Bo, Zhang Guixin, Li Chengrong, et al. Research status and prospect of gas-insulated metal enclosed transmission line[J]. High Voltage Engineering,2015,41(5):1466-1473.

张彬,张周胜,于瑞冬,等.直流均匀电场下金属微粒运动状态与识别[J].电力科学与技术学报,2025,40(1):265-273.

Zhang Bin, Zhang Zhousheng, Yu Ruidong, et al.Motion state and identification of metal particles in a uniform DC electric field[J].Journal of Electric Power Science And Technology,2025,40(1):265-273.

杨帆,高有华.Mayr电弧模型下GIS中快速暂态过电压的仿真分析[J].电器与能效管理技术,2024,(2):28-32.

Yang Fan, Gao Youhua.Simulation analysis of fast transient overvoltage in GIS under Mayr arc model[J]. 2024,(2):28-32.

DL/T 916—2005 六氟化硫气体酸度测定法[S].

DL/T 916—2005 Determination of acidity in sulphur hexafluoride[S].

DL/T 918—2005 六氟化硫气体中可水解氟化物含量测定法[S].

DL/T 918—2005 Determination of hydrolyzable fluoride content in sulfur hexafluoride gas[S].

DL/T 919—2005 六氟化硫气体中矿物油含量测定法(红外光谱分析法)[S].

DL/T 919—2005 Determination of mineral oil content in sulphur hexafluoride by infrared spectrum method[S].

国家电网公司,江苏省电力公司,江苏省电力公司电力科学研究院,山东中惠仪器有限公司.一种六氟化硫气体中可水解氟化物含量标准气的配制装置及方法: CN104793277A[P]. 2015-07-22.

State Grid Corporation of China, Jiangsu Electric Power Company, Jiangsu Electric Power Research Institute, Shandong Zhonghui Instrument Co. , Ltd. A preparation device and method for a standard gas with specified hydrolyzable fluoride content in sulfur hexafluoride: CN104793277A[P]. 2015-07-22.

国家电网公司,江苏省电力公司,江苏省电力公司电力科学研究院,山东中惠仪器有限公司.一种SF 6 气体中矿物油含量标准气的配制装置及方法: CN104807682A[P ] . 2015-07-29.

State Grid Corporation of China, Jiangsu Electric Power Company, Jiangsu Electric Power Research Institute, Shandong Zhonghui Instrument Co. , Ltd. A preparation device and method for a standard gas of mineral oil content in SF 6 gas: CN104807682A[P ] . 2015-07-29.

浏览量

下载量

CSCD

文章被引用时，请邮件提醒。

提交

工具集

关联资源

喷口烧蚀对SF6开关设备电弧放电分解产物的影响研究

基于VSG的并网变流器惯量阻尼综合自适应控制

750 kV架空地线感应电流及损耗影响规律研究

油纸绝缘系统过热故障油面气体产气规律研究

真空断路器分闸电磁铁动态仿真及故障分析